KJL Sputter is one of the methods to do Physical Vapor Deposition (PVD). To my knowledge, there are mainly two ways to do PVD in the cleanroom: evaporator and sputter.
- loading smaple
- close the vacuum valve
- turn off “Turbo Pump”
- wait for 1 min. (this is to protect turbo pump)
- open N2 gas valve slowly to vent the loadlock
- leave the loadlock latch open. The loadlock latch will open automatically when N2 gas is full inside the loading chamber.
- close the N2 gas valve
- load the wafer to the holder (Groove towards “upside”)
- close the loadlock latch
- check whether “backing pump” is working or not. If not, turn on the “backing pump” first.
- check whether “turbo pump” is turned off. It should be “zero” before opening “vacuum valve”.
- open the “vacuum valve”.
- When the pressure reaches to 2.5e-1 Torr, turn on “turbo pump”.
(Xiaoyu don’t put too much detailed information; Yoonho explains detailed information. Please refer to Yoonho’s notes if you want to know detailed information.)
2.Transferring sample
- When the pressure reaches to 6.0e-6 Torr, open the “Gate Valve”.
- Push inside the wafer docking port using a loading bar
- Pull out the wafer docking port using a loading bar
- close the “Gate Valve”
3.Initiate Plasma – pre-sputtering process (Ti)
- close the throttle valve until it touches screw knob
- rotate screw gauage to indicate ~9 grade
- turn up the Ar gas knob
- wait until the gas rate is stabilized
- check the MFC display and Modify the gas flow rate
- If you want to set the gas flow rate, then move “READOUT SELECT” knob to “SET” and Change the value and Move the knob to “READ”
- Turn the “PLANETARY CONTROL” On and Set the “Speed” as 20 rpm (Rotate your sample) (display value : 20)
- Maintain the chamber pressure around from 25 ~ 30mTorr
- Turn on the “POWER” and Turn on “OUPUT” on the “Power Supply”
- Increase the power up to “150W” using “LEVEL” knob
- When the power doesn`t go up even though you rotate “LEVEL” knob, then
- Increase the gas flow rate from 50 to 90 sccm
- Increase the gas flow rate from 50 to 90 sccm
- Decrease the chamber pressure to 7.8mTorr by Rotating screw gauage ~7.6
4.Main sputtering process (Ti)
- Increase the power up to 300W using “LEVEL” knob for Ti deposition
- Set time using your personal timer
- Open the shutter and Start your personal timer
- * 2min deposition yields 28nm Ti layer (Deposition rate : 14nm/min)
- After deposition, Close the shutter – Decrease the power to 0W
- Turn off the “OUTPUT” and Turn off the “POWER” on the “Power Supply”
- Turn the gas knob “Down” position
- Open the throttle value fully –
- Wait for 2min
5.Pre-sputtering process (Pt)
- Close the throttle valve until it touches screw knob
- Rotate screw gauage to indicate ~9 grade
- Turn the gas knob “Up” position
- Wait until the gas rate is stabilized
- Maintain the chamber pressure around 30mTorr
- Turn on “POWER” on the Tunner
- Turn on “POWER”
- Turn on “RF ON”
- Increase power level to “50W”
- Open shutter for 1s and Close the shutter to make sure initiating plasma
- Increase the power level to “150W”
- Decrease the chamber pressure to 7.8mTorr by Rotating screw gauage ~7.6
6.main-sputtering process (Pt)
- Increase the power up to 300W using “LEVEL” knob for Pt deposition
- Set time using your personal timer
- Open the shutter and Start your personal timer
- 4min 30s deposition yields 100nm Pt layer
- After deposition, Close the shutter
- Decrease the power to 0W
- Turn off the “RF ON” and Turn off the “POWER”
- Turn the gas knob “Down” position
- Turn the “PLANETARY CONTROL” Off
- Open the throttle value fully
- Wait for 2min
7.transferring sample
- Open the “Gate Valve”
- Push inside the wafer docking port using a loading bar (Groove should be towards “downside”)
- Unload the wafter docking port from the rail in the main chamber
- Pull out the wafer docking port using a loading bar
- Close the “Gate Valve”
8.unloading sample
- Close the “Vacuum valve”
- Turn off “Turbo Pump”
- Wait for 1min
- Open the N2 gas valve slowly to vent the loadlock
- Loadlock will automatically be open
- Close the N2gas valve
- Unload your sample from that wafer docking port
- Close the Loadlock latch
- Check whether “Turbo pump” is turned off (It should be “zero” before opening “Vacuum valve”)
- Open the “Vacuum valve”
- Turn on “Turbo pump” when pressure reaches to 2.5e-1 Torr
You can leave now 🙂
Chamber opening
- Hi-Vac Valve off
- Chamber Vent Valve on
- When the ATM is on, turn off Chamber vent valve off
- Hoist “up”
Chamber closing
- Hoist “down”
- Rough valve on
- When the chamber process reaches to 50mTorr, turn off Rough valve
- Turn on Hi-Vac valve
Trouble shooting
- RF power supply case
- If the Forward power directly goes up high and fluctuate? -> Check your power knob was all the way to 0.
- the main chamber pressure cannot go down to 30 mTorr
- double check the “CRYO PUMP” is on
- double check the “HI-VAC” is on